Influence of Curing Methods on Properties of Composite Restoratives

Objectives: the aim of this study was to verify the influence of curing methods on contraction stress, stress rate, degree of conversion (DC), volumetric shrinkage (VS) of a restorative composite and on bond strength of composite restoratives. Methods: for the stress test, composite (0.84 mm thick) was applied between two 5-mm diameter glass rods, mounted in a servohydraulic machine. Stress rate was taken by the value of stress/time at each second. DC was measured by micro-FTIR and VS by mercury dilatometer. Bond strength testing was performed using a push-out test. The C-factor in all tests was 3.0. Four curing methods were tested: Continuous Light (CL), Soft-Start (SS), and two Pulse Delay methods using different initial irradiances - 150 (PD150) and 80 mW/cm2 (PD80). Results were analyzed by ANOVA and Tukey's test (a = 0.05). Results: stress values ranged from 7.9 MPa (PD80) to 10.3 MPa (CL). No statistical difference was observed among CL, SS, and PD150. PD80 presented statistically lower stress values compared to CL and SS. CL presented the highest maximum stress rate, followed by SS, PD150 and PD80. Mean DC values ranged from 54.2% (PD150) to 55.9% (PD80) and mean VS values ranged from 2.02% (PD150) to 2.29% (SS), with no statistical difference among the curing methods for both tests. For the bond strength test, values ranged from 26.4 MPa (CL) to 35.5 MPa (PD150). PD150 and PD80 were both statistically superior to SS and CL. SS presented statistically higher bond strength compared to CL. Conclusion: modulated curing methods were shown to be effective in reducing contraction stress rate and improving the strength of the bonded interface, and without compromising the DC of the restorative composite. Supported by CAPES (Brazil - PDEE grants BEX3428/04-4).